Differential Scanning Calorimetry RB /18/2017

Transcription

1 Differential Scanning Calorimetry Rebar Size Sales Order Date Produced RB Work Order /18/2017 Formulation Line Speed RBVEIP RPM - 44 Neat Resin Tg C Formulated Resin Tg C Neat Resin Per ASTM E (Reapproved 2014) ASTM E (Reapproved 2012) Ave Resin % Formulated Resin = 1 - (ΔH Residual Cure / ΔH Full Cure) * ΔH Full Cure Line / Sample 1 Line / Sample 2 Line / Sample 3 Line / Sample 4 Tf Onset 99.3 C 97.3 C 97.0 C 97.3 C Tg Tm or Tig C C C C Sample Weight (mg) Reported ΔH Residual Cure Corrected Residual Enthalpy Calculated 99.36% 99.54% 99.40% 99.09% The values in the above fields are taken or calculated from the DSC scans which are attached as icons in the Chart fields DSC Chart 1 DSC Chart 2 DSC Chart 3 DSC Chart 4 DSC Chart 5 DSC Calibration DSC Verification DSC Report Hughes Brothers, Inc. Seward, NE

2 Sample: RB4 WO Line 1 Size: mg Method: 10 C per Minute Ramp Comment: Q2000, 50 ml/min Ni, Tzero AL Pan 0.1 DSC File: \\...\Rebar\RB6\RB6 WO Line Operator: R Kruse Run Date: 26 Jan :00 Instrument: DSC Q2000 V24.11 Build Heat Flow (W/g) C C(H) C C C J/g Deriv. Heat Flow (W/(g C)) Exo Up Temperature ( C) Universal V4.5A TA Instruments

3 Differential Scanning Calorimetry Rebar Size Sales Order Date Produced RB Work Order /31/2017 Formulation Line Speed RBVEIP rpm - 65 Neat Resin Tg C Formulated Resin Tg C Neat Resin Per ASTM E (Reapproved 2014) ASTM E (Reapproved 2012) Ave Resin % Formulated Resin = 1 - (ΔH Residual Cure / ΔH Full Cure) * ΔH Full Cure Line / Sample 1 Line / Sample 2 Line / Sample 3 Line / Sample 4 Tf Onset C C C C Tg Tm or Tig C C C C Sample Weight (mg) Reported ΔH Residual Cure Corrected Residual Enthalpy Calculated 98.72% 98.30% 97.82% 98.71% The values in the above fields are taken or calculated from the DSC scans which are attached as icons in the Chart fields DSC Chart 1 DSC Chart 2 DSC Chart 3 DSC Chart 4 DSC Chart 5 DSC Calibration DSC Verification DSC Report Hughes Brothers, Inc. Seward, NE

4 Sample: RB4 WO Line 1 Size: mg Method: 10 C per Minute Ramp Comment: Q2000, 50 ml/min Ni, Tzero AL Pan 0.05 DSC File: \\...\RB4\RB4 WO Line 1x.001 Operator: R Kruse Run Date: 06 Feb :58 Instrument: DSC Q2000 V24.11 Build Heat Flow (W/g) Deriv. Heat Flow (W/(g C)) C C(H) C C J/g 0.20 Exo Up C Temperature ( C) Universal V4.5A TA Instruments

5 Differential Scanning Calorimetry Rebar Size Sales Order Date Produced RB5 Work Order /16/2017 Formulation Line Speed RBVEIP Rpm Neat Resin Tg Formulated Resin Tg C Neat Resin Per ASTM E (Reapproved 2014) ASTM E (Reapproved 2012) Ave Resin % Formulated Resin = 1 - (ΔH Residual Cure / ΔH Full Cure) * ΔH Full Cure Line / Sample 1 Line / Sample 2 Line / Sample 3 Line / Sample 4 Tf Onset C C C 98.4 C Tg Tm or Tig C C C C Sample Weight (mg) Reported ΔH Residual Cure Corrected Residual Enthalpy Calculated 98.80% 99.67% 98.89% 98.15% The values in the above fields are taken or calculated from the DSC scans which are attached as icons in the Chart fields DSC Chart 1 DSC Chart 2 DSC Chart 3 DSC Chart 4 DSC Chart 5 DSC Calibration DSC Verification DSC Report Hughes Brothers, Inc. Seward, NE

6 Sample: RB5 WO Line2 Size: mg Method: 10 C per Minute Ramp Comment: Q2000, 50 ml/min N2, Tzero Al Pan 0.05 DSC File: \\...\Rebar\RB5\RB5 WO Line Operator: R Kruse Run Date: 24 May :46 Instrument: DSC Q2000 V24.11 Build Heat Flow (W/g) Deriv. Heat Flow (W/(g C)) C C(H) C C C J/g 0.20 Exo Up Temperature ( C) Universal V4.5A TA Instruments

7 Differential Scanning Calorimetry Rebar Size Sales Order Date Produced RB8 Work Order /20/2016 Formulation Line Speed RBVEIP rpm - 33 Neat Resin Tg C Formulated Resin Tg C Neat Resin Per ASTM E (Reapproved 2014) ASTM E (Reapproved 2012) Ave Resin % Formulated Resin = 1 - (ΔH Residual Cure / ΔH Full Cure) * ΔH Full Cure Line / Sample 1 Line / Sample 2 Line / Sample 3 Line / Sample 4 Tf Onset C C C C Tg Tm or Tig C C C C Sample Weight (mg) Reported ΔH Residual Cure Corrected Residual Enthalpy Calculated 98.71% 99.59% 99.15% 98.23% The values in the above fields are taken or calculated from the DSC scans which are attached as icons in the Chart fields DSC Chart 1 DSC Chart 2 DSC Chart 3 DSC Chart 4 DSC Chart 5 DSC Calibration DSC Verification DSC Report Hughes Brothers, Inc. Seward, NE

8 Sample: RB8 WO Line 1 Size: mg Method: 10 C per Minute Ramp Comment: Q2000, 50 ml/min Ni, Tzero AL Pan 0.05 DSC File: \\...\Rebar\RB8\RB8 WO Line Operator: R Kruse Run Date: 11 Jan :04 Instrument: DSC Q2000 V24.11 Build Heat Flow (W/g) Deriv. Heat Flow (W/(g C)) C C(H) C C C J/g Exo Up Temperature ( C) Universal V4.5A TA Instruments